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Standard [CURRENT]

DIN EN 15510:2017-10

Animal feeding stuffs - Methods of sampling and analysis - Determination of calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead by ICP-AES; German version EN 15510:2017

German title
Futtermittel - Probenahme- und Untersuchungsverfahren - Bestimmung von Calcium, Natrium, Phosphor, Magnesium, Kalium, Eisen, Zink, Kupfer, Mangan, Cobalt, Molybdän und Blei mittels ICP-AES; Deutsche Fassung EN 15510:2017
Publication date
2017-10
Original language
German
Pages
35

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Publication date
2017-10
Original language
German
Pages
35
DOI
https://dx.doi.org/10.31030/2666145

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Overview

DIN EN 15510 specifies the inductively coupled plasma atomic emission spectroscopy (ICP-AES) method for the determination of the elements calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead. The elements calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt, molybdenum and lead are extracted either in feeds mainly consisting of organic matter after dry ashing and dissolving in hydrochloric acid or in feeds mainly consisting of inorganic matter after wet digestion with hydrochloric acid. For the determination of extractable lead in minerals and feeds containing phyllosilicates (for example, kaolinite clay) wet digestion with diluted nitric acid should be used. The method was successfully tested for: - calcium, sodium, phosphorus, magnesium, potassium, iron, zinc, copper, manganese, cobalt and molybdenum in the following animal feeding stuffs: 2 complete feeds (pig feed, sheep feed), 1 feed material (phosphate), 1 mineral premixture and 2 complementary feeds (2 mineral feeds), - lead in 2 feed materials (phosphate, CaCO3), 2 feed additives (Bentonite, CuSO4), 1 complementary feed (mineral feed). For elements with a HORRAT value higher than 2 (see Annex A) the method is more applicable as a screening method and not for confirmatory purposes. The method detection limit for each element is dependent on the sample matrix and the instrument. The method is not applicable for the determination of a low concentration of elements. The limit of quantification should be 3 mg/kg or lower. The European Standard has been prepared by CEN/TC 327 "Animal feeding stuffs - Methods of sampling and analysis", the secretariat of which is held by NEN (Netherlands). The responsible German standardization committee is Working Committee NA 057-03-03 AA "Futtermittel" ("Animal feeding stuffs") at DIN Standards Committee Food and Agricultural Products (NAL).

Content
ICS
65.120
DOI
https://dx.doi.org/10.31030/2666145
Replacement amendments

This document replaces DIN EN 15510:2007-10 .

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