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Standard [CURRENT]

DIN EN ISO 13196:2015-11

Soil quality - Sreening soils for selected elements by energy-dipersive X-ray fluorescence spectrometry using a handheld or portable instrument (ISO 13196:2013); German version EN ISO 13196:2015

German title
Bodenbeschaffenheit - Screening ausgewählter Elemente in Böden mit handhaltbaren oder tragbaren Röntgenfluoreszenzspektrometern (ISO 13196:2013); Deutsche Fassung EN ISO 13196:2015
Publication date
2015-11
Original language
German
Pages
21

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Publication date
2015-11
Original language
German
Pages
21
DOI
https://dx.doi.org/10.31030/2337983

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Overview

This International Standard specifies the procedure for screening soils and soil-like materials for selected elements when handheld or portable energy-dispersive XRF spectrometers are used. This quick method is assumed to be applied on-site to obtain qualitative or semiquantitative data that assists decisions on further sampling strategy for assessing soil quality. The higher the efforts for pretreatment used on soil samples, the better the analytical results can be expected. This International Standard does not explicitly specify elements for which it is applicable, since the applicability depends on the performance of the apparatus and the objective of the screening. The elements which can be determined are limited by the performance of the instruments used, the concentration of the element present in the soil, and the requirements of the investigation (for example guideline value). For Hg, Cd, Co, Mo, V and Sb, a majority of instruments are not sensitive enough to reach sufficiently low limits of quantification (LOQ) to meet the requirements (limit or threshold values) set in the ordinances of different countries. In this case, other methods need to be employed to measure these low concentrations. Usually, wet chemical methods are used, based on aqua regia extracts, in combination with optical or mass spectrometric (MS) methods like atomic absorption spectrometry (AAS), inductively coupled plasma-optical emission spectrometry (ICP-OES) or ICP-MS.

Content
ICS
13.080.10
DOI
https://dx.doi.org/10.31030/2337983

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